LOW CRYSTALLINITY NANOHYDROXYAPATITE PREPARED AT ROOM TEMPERATURE

Aurora  MOCANU; Reka  BALINT; Corina  ISTRATE (GARBO); Lucia Iacobina  TIMIȘ; Ioan  PETEAN; Ossi  HOROVITZ; Maria  TOMOAIA-COTISEL

doi:10.24193/subbchem.2017.2.07

LOW CRYSTALLINITY NANOHYDROXYAPATITE PREPARED AT ROOM TEMPERATURE

Authors

Aurora MOCANU Research Center of Physical Chemistry, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: aurora.mocanu@ubbcluj.ro. https://orcid.org/0000-0002-8728-045X
Reka BALINT Research Center of Physical Chemistry, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: reka.balint@ubbcluj.ro. https://orcid.org/0000-0003-2395-116X
Corina ISTRATE (GARBO) Research Center of Physical Chemistry, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: maria.tomoaia@ubbcluj.ro. https://orcid.org/0000-0002-7934-103X
Lucia Iacobina TIMIȘ Department of Odontology, Faculty of Dentistry, Iuliu Hațieganu University of Medicine and Pharmacy, Cluj-Napoca, Romania. Email: timis.lucia@umfcluj.ro.
Ioan PETEAN Research Center of Physical Chemistry, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: ipetean@chem.ubbcluj.ro. https://orcid.org/0000-0003-3274-8817
Ossi HOROVITZ Research Center of Physical Chemistry, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Corresponding author: mocanu.aurora@gmail.com. https://orcid.org/0000-0002-3652-8558
Maria TOMOAIA-COTISEL Research Center of Physical Chemistry, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: maria.tomoaia@ubbcluj.ro. https://orcid.org/0000-0002-0995-3006

DOI:

https://doi.org/10.24193/subbchem.2017.2.07

Keywords:

nanohydroxyapatite, chemical synthesis, XRD, TEM, AFM, FTIR, BET

Abstract

In order to obtain a low crystalline nanohydrxyapatite (HAP), suitable for biomedical application, a new synthesis procedure was developed, based on the aqueous precipitation method, at room temperature, without any additives. Accordingly, lyophilized HAP powders, both calcined and non calcined, were prepared, and characterized by XRD, TEM and AFM imaging, FTIR spectroscopy, zeta potential and BET measurements. The results confirmed HAP as the only phase present. The high porosity of this nanomaterial is attained. The nanoparticle size and shape as well as the crystallinity degree of the obtained HAP samples were also determined.

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STUDIA UBB CHEMIA, Volume 62 (LXII), No. 2, Tome I, June 2017

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Published

2017-06-01

How to Cite

MOCANU, A. ., BALINT, R. ., ISTRATE (GARBO), C. ., TIMIȘ, L. I. ., PETEAN, I. ., HOROVITZ, O. ., & TOMOAIA-COTISEL, M. . (2017). LOW CRYSTALLINITY NANOHYDROXYAPATITE PREPARED AT ROOM TEMPERATURE. Studia Universitatis Babeș-Bolyai Chemia, 62(2), 95–103. https://doi.org/10.24193/subbchem.2017.2.07