PARACETAMOL DETECTION AT A GRAPHITE PASTE MODIFIED ELECTRODE BASED ON PLATINUM NANOPARTICLES IMMOBILISED ON Al-SBA-15 COMPOSITE MATERIAL

Thi Thanh Hien NGO; Carmen Ioana FORȚ (LADIU); Thanh Huyen PHAM; Graziella Liana TURDEAN

doi:10.24193/subbchem.2020.1.03

PARACETAMOL DETECTION AT A GRAPHITE PASTE MODIFIED ELECTRODE BASED ON PLATINUM NANOPARTICLES IMMOBILISED ON Al-SBA-15 COMPOSITE MATERIAL

Authors

Thi Thanh Hien NGO HaNoi University of Science and Technology, School of Chemical Engineering, 1 Dai Co Viet, Hanoi, Vietnam
Carmen Ioana FORȚ (LADIU) Department of Chemical Engineering, Faculty of Chemistry and Chemical Engineering, Babes-Bolyai University; Institute of Research-Development-Innovation in Applied Natural Sciences, Babes-Bolyai University, Cluj-Napoca, Romania. Email: iladiu@chem.ubbcluj.ro. https://orcid.org/0000-0002-4675-7602
Thanh Huyen PHAM HaNoi University of Science and Technology, School of Chemical Engineering, 1 Dai Co Viet, Hanoi, Vietnam. *Corresponding author: huyen.phamthanh@hust.edu.vn https://orcid.org/0000-0002-2115-811X
Graziella Liana TURDEAN “Babeş-Bolyai” University, Faculty of Chemistry and Chemical Engineering, Department of Chemical Engineering, 11 Arany Janos St., 400028 Cluj-Napoca, Romania. *Corresponding author: gturdean@chem.ubbcluj.ro https://orcid.org/0000-0003-1273-6878

DOI:

https://doi.org/10.24193/subbchem.2020.1.03

Keywords:

Pt nanoparticles, ordered mesoporous structure, graphite paste modified electrode, paracetamol

Abstract

A composite material was obtained by immobilizing platinum nanoparticles (Pt-NPs) within an ordered mesoporous structure Al-SBA15 (having improved acidity due to the presence of Al). This was used for preparing a graphite paste modified electrode (Pt/Al-SBA-15-GPE), which was applied for paracetamol (PA) detection. The obtained electrode was investigated by electrochemical methods (e.g. cyclic voltammetry, CV and electrochemical impedance spectroscopy, EIS), in order to estimate the electrochemical parameters, which were compared with those of GPE unmodified electrode. Square-wave voltammetry (SWV) was used to obtain the analytical parameters of Pt/Al-SBA-15-GPE for PA detection. The good analytical parameters recommend the composite mesoporous material (Pt/Al-SBA-15) to be used for preparing modified electrodes for PA detection in real samples.

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STUDIA UBB CHEMIA, Volume 65 (LXV), No. 1, March 2020

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Published

2020-03-20

How to Cite

NGO, T. T. H., FORȚ (LADIU), C. I., PHAM, T. H., & TURDEAN, G. L. (2020). PARACETAMOL DETECTION AT A GRAPHITE PASTE MODIFIED ELECTRODE BASED ON PLATINUM NANOPARTICLES IMMOBILISED ON Al-SBA-15 COMPOSITE MATERIAL. Studia Universitatis Babeș-Bolyai Chemia, 65(1), 27–38. https://doi.org/10.24193/subbchem.2020.1.03