INVESTIGATION OF THE FUNCTIONAL LAYER FORMATION ON THE SURFACE OF CARBON MATERIAL

Authors

  • Saken ABDIMOMYN Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan https://orcid.org/0000-0002-5985-9050
  • Azhar ATCHABAROVA Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan. atchabarova.azhar@kaznu.kz https://orcid.org/0000-0002-4600-2728
  • Dinara ABDUAKHYTOVA Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan
  • Rustam TOKPAYEV Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan https://orcid.org/0000-0002-0117-4454
  • Kanagat KISHIBAYEV Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan https://orcid.org/0000-0003-1590-5243
  • Tamina KHAVAZA Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan https://orcid.org/0000-0002-1614-3060
  • Andrey KURBATOV Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan https://orcid.org/0000-0003-1883-310X
  • Graziella Liana TURDEAN Babeş-Bolyai University, Faculty of Chemistry and Chemical Engineering, 11 Arany Janos str., RO-400028, Cluj-Napoca, Romania. gturdean@chem.ubbcluj.ro https://orcid.org/0000-0003-1273-6878
  • Mikhail NAURYZBAYEV Center of Physical Chemical Methods of Research and Analysis, al-Farabi Kazakh National University, Almaty, Kazakhstan https://orcid.org/0000-0002-6781-6464

DOI:

https://doi.org/10.24193/subbchem.2022.4.10

Keywords:

hydrothermal carbonization, carbon material, thermal carbonization, walnut shell, activated carbon, functional layer.

Abstract

In this study, a comparison of walnut-based carbon materials (CM) obtained by hydrothermal carbonization (HTC) and HTC in combination with steam gas activation (SGA) was carried out. In order to study the effect of steam activation on the functional layer formation, the obtained materials were studied by SEM, nitrogen adsorption/desorption by Brunauer-Emmett-Teller (BET) method, Raman spectroscopy, X-ray diffraction spectroscopy (XRD), X-ray fluorescence elemental analysis (XRF). Functional groups (FG) were evaluated qualitatively and quantitatively by Fourier transform infrared spectroscopy (FTIR), acetone extract analysis of CM by gas chromatography-mass spectrometry (GC-MS), and potentiometrically Boehm titration. The described mechanism of the influence of the base nature on the surface functionality correlates well with the results of the powder addition method. The HTC or HTC+SGA treatment provides a wide range of possibilities for further controlled modification of the carbon sorbent surface for specific adsorption purposes.

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STUDIA UBB CHEMIA, Volume 67 (LXVII), No. 4, December 2022

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Published

2022-12-30

How to Cite

ABDIMOMYN, S., ATCHABAROVA, A., ABDUAKHYTOVA, D., TOKPAYEV, R., KISHIBAYEV, K., KHAVAZA, T., … NAURYZBAYEV, M. (2022). INVESTIGATION OF THE FUNCTIONAL LAYER FORMATION ON THE SURFACE OF CARBON MATERIAL. Studia Universitatis Babeș-Bolyai Chemia, 67(4), 151–167. https://doi.org/10.24193/subbchem.2022.4.10

Issue

Volume 67, No. 4, 2022

Section

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