NEW STANNEPINE DERIVATIVES. SYNTHESIS AND CHARACTERISATION

Authors

  • Lavinia BUTA Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Corresponding author: sgabi@chem.ubbcluj.ro. https://orcid.org/0000-0002-7171-0574
  • Raluca SEPTELEAN Department of Chemical Engineering, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: sraluca@chem.ubbcluj.ro. https://orcid.org/0000-0003-3458-8394
  • Noémi DEAK Facultatea de Chimie şi Inginerie Chimică, Universitatea Babeş-Bolyai, Cluj-Napoca, Romania; UPS, LHFA, Université de Toulouse, France, CNRS, LHFA, Toulouse, France. Email: noemideak@chem.ubbcluj.ro. https://orcid.org/0000-0002-9401-0298
  • Alexandra POP Department of Chemistry, Supramolecular Organic and Organometallic Chemistry Centre (SOOMCC), Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: alexandra.m.pop@ubbcluj.ro. https://orcid.org/0000-0002-2355-3682
  • Gabriela NEMES Department of Chemical Engineering, Faculty of Chemistry and Chemical Engineering, Babeş-Bolyai University, Cluj-Napoca, Romania. Email: gabriela.nemes@ubbcluj.ro.

Keywords:

diphenylstannepine, dibromostilbene, dihalostannepine

Abstract

A new diphenylstannepinic derivative has been synthesized and completely characterized in solution and in solid state (multinuclear NMR spectroscopy, HRMS, X-ray diffraction). As a result of the reaction of the diphenylstannepinic derivative with bromine, a brominated product was evidenced by NMR spectroscopy.

References

P.P. Power, Chemical Reviews, 1999, 99, 3463.

B.E. Eichler, D.R. Power, R. West, Organometallics, 1998, 17(11), 2147.

J. Escudie, H. Ranaivonjatovo, L. Rigon, Chemical Reviews, 2000, 100, 3639.

V.Y. Lee, A. Seckiguchi, Organometallics compounds of low coordinated Si, Ge, Sn and Pb, 2010, John Wiley &Sons Ltd, West Sessex, U.K,

ISBN: 978-0-470-72543-6.

J. Escudie, G. Nemes, Comptes Rendus de Chimie, 2010, 13, 954.

T.G. Kocsor, D. Matioszek, G. Nemes, A. Castel, Annie, J. Escudie, P.M. Petrar, N. Saffon-Merceron, I. Haiduc, Inorganic Chemistry, 2012, 51, 7782.

T.G. Kocsor, G. Nemes, N. Saffon, S. Mallet-Ladeira, D. Mandec, A.Castel,

J. Escudie, Dalton Transactions, 2014, 43, 2718.

R. Septelean, G. Nemes, J Escudie, I. Silaghi-Dumitrescu, H. Ranaivonjatovo, P. Petrar, H. Gornitzka, L. Silaghi-Dumitrescu, N. Saffon, European Journal of Inorganic Chemistry, 2009, 5, 628.

P.M. Petrar, R. Septelean, N. Deak, H. Gornitzka, G. Nemes, Journal of Organometalic Chemistry, 2015, 787, 14.

T.G. Kocsor, N. Deak, D. Ghereg, G. Nemes, J. Escudié, H. Gornitzka, S. Ladeira, A. Castel, Journal of Organometalic Chemistry, 2014, 755, 1204.

A. Caruso, A.M. Siegler, J.D. Tovar, Angewandte Chemie International Edition, 2010, 49, 4213.

R. Septelean, G. Nemes, P.M. Petrar, Revue Roumaine de Chimie, 2014, 59 (11-12), 997.

S.S. Batsanov, Inorganic Materials, 2001, 9, 871.

E.R.T. Tiekink, J. Zukerman-Schpector, The Importance of Pi-Interactions in Crystal Engineering, 2012, John Wiley & Sons Ltd, The Atrium, Southern Gate, Chichester, West Sussex, PO19 8SQ, U. K. ISBN 978-0-470-68827-4.

E. Gagnon, A. Rochefort, V. Metivaud, J. D. Wuest, Organic Letters, 2010, 12, 380.

D. Dakternieks, K. Jurkschat, R. Tozer, Organometallics, 1996, 1467.

A. Terfort, H. Brunner, Journal of the Chemical Society, Perkin Transaction 1, 1996, 1467.

G.M. Sheldrick, SHELX-97, Universität Göttingen, Germany, 1997.

DIAMOND – Visual Crystal Structure Information System, CRYSTAL IMPACT: Bonn, Germany, 2001.

STUDIA UBB CHEMIA, Volume 61 (LXI), No. 3, September 2016

Downloads

Published

2016-09-30

How to Cite

BUTA, L. ., SEPTELEAN, R., DEAK, N., POP, A. ., & NEMES, G. . (2016). NEW STANNEPINE DERIVATIVES. SYNTHESIS AND CHARACTERISATION. Studia Universitatis Babeș-Bolyai Chemia, 61(3), 81–90. Retrieved from https://studia.reviste.ubbcluj.ro/index.php/chemia/article/view/8333

Issue

Volume 61, No. 3, Tome I, 2016

Section

Articles

License

Copyright (c) 2016 Studia Universitatis Babeș-Bolyai Chemia

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.

Most read articles by the same author(s)