GRAPHITE PASTE ELECTRODE MODIFIED WITH  ZEOLITIC IMIDAZOLATE FRAMEWORK (ZIF-67)  FOR THE DETERMINATION OF ACETAMINOPHEN

Thi Thanh Hien NGO; Thi Hai Yen PHAM; Nguyen Thoai DANG; Thi Vuong Hoan NGUYEN; Thanh Huyen PHAM; Graziella Liana TURDEAN

doi:10.24193/subbchem.2023.1.01

GRAPHITE PASTE ELECTRODE MODIFIED WITH ZEOLITIC IMIDAZOLATE FRAMEWORK (ZIF-67) FOR THE DETERMINATION OF ACETAMINOPHEN

Authors

Thi Thanh Hien NGO Quy Nhon University, Faculty of Natural Sciences, 170 An Duong Vuong, Quy Nhon 55000, Vietnam
Thi Hai Yen PHAM Institute of Chemistry, Vietnam Academy of Science Technology, 18 Hoang Quoc Viet, Cau Giay, Hanoi 100000, Vietnam
Nguyen Thoai DANG Quy Nhon University, Faculty of Natural Sciences, 170 An Duong Vuong, Quy Nhon 55000, Vietnam https://orcid.org/0000-0003-4368-2841
Thi Vuong Hoan NGUYEN Quy Nhon University, Faculty of Natural Sciences, 170 An Duong Vuong, Quy Nhon 55000, Vietnam
Thanh Huyen PHAM Ha Noi University of Science and Technology, School of Chemical Engineering, 1 Dai Co Viet, HaNoi 100000, Vietnam https://orcid.org/0000-0003-3669-8079
Graziella Liana TURDEAN Babes-Bolyai University, Faculty of Chemistry and Chemical Engineering, Department of Chemical Engineering, Center of Electrochemistry and Non-conventional Materials, 11 Arany Janos, 400198 Cluj-Napoca, Romania. graziella.turdean@ubbcluj.ro https://orcid.org/0000-0003-1273-6878

DOI:

https://doi.org/10.24193/subbchem.2023.1.01

Keywords:

Zeolitic imidazolate framework, graphite paste modified electrode, acetaminophen

Abstract

A zeolitic imidazolate framework ZIF-67 was synthesized by an eco-friendly solvothermal method, using ethanol as solvent at room temperature. The morphology and structure of obtained ZIF-67 were characterized by X-ray diffraction, scanning electron microscopy (SEM), nitrogen adsorption/desorption isotherm, energy dispersive spectroscopy (EDS), and Fourier-transform infrared spectroscopy (FTIR). The ZIF-67 modified graphite paste electrode (ZIF-67-GPE) was prepared and used for the electrochemical detection of acetaminophen (AC). Cyclic voltammetry (CV) and square wave voltammetry (SWV) were employed to investigate the electrochemical behavior of AC at ZIF-67-GPE modified electrode. At the optimal working conditions, the limit of detection was 0.2 μM (S/N = 3) in the linear range of 2 - 10 μM AC. The good analytical parameters indicated its applicability for AC determination in real samples.

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STUDIA UBB CHEMIA, Volume 68 (LXVIII), No. 1, March 2023

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Published

2023-03-27

How to Cite

NGO, T. T. H., PHAM, T. H. Y., DANG, N. T., NGUYEN, T. V. H., PHAM, T. H., & TURDEAN, G. L. (2023). GRAPHITE PASTE ELECTRODE MODIFIED WITH ZEOLITIC IMIDAZOLATE FRAMEWORK (ZIF-67) FOR THE DETERMINATION OF ACETAMINOPHEN. Studia Universitatis Babeș-Bolyai Chemia, 68(1), 7–17. https://doi.org/10.24193/subbchem.2023.1.01